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Ring Chain Transformations. XIV. 3-(omega-Aminoalkyl)-1,2,4-triazoles by Reaction of Isothiosemicarbazides with Lactam Acetals or Lactim Ethers
Isothiosemicarbazide hydrohalides 1 react with lactam acetals 2 or lactim ethers 3 by the formation of lactamisothiosemicarbazones 4 or ring transformed 3-(omega-aminoalkyl)-1,2,4-triazoles 6.The latter can independently by synthesized by alkylation of lactamthiosemicarbazones 9.Condensation of primary 3-(omega-aminoalkyl)-1,2,4-triazoles 6 with lactim ethers 7 can lead to 3-lactamiminoalkyl-1,2,4-triazoles 8.
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Reference£º
Pyrroline – Wikipedia,
1-Pyrroline | C4H7N – PubChem