The prevalence of solvent effects in heterogeneous catalysis in condensed media has motivated developing quantitative kinetic, spectroscopic, and theoretical assessments of solvent structures and their interactions with reaction intermediates. 5306-85-4, Name is (3R,3aR,6S,6aR)-3,6-Dimethoxyhexahydrofuro[3,2-b]furan, molecular formula is C8H14O4, belongs to pyrrolines compound, is a common compound. In a patnet, author is Woydziak, ZR, once mentioned the new application about 5306-85-4, Name: (3R,3aR,6S,6aR)-3,6-Dimethoxyhexahydrofuro[3,2-b]furan.
Unusual tosyl transfer solvolysis reaction to 3-n-butyl-4-methyl-5,5-di-p-toluenesulfonyl-3-pyrrolin-2-one
The title compound (1) was isolated in 20-30% recovery following solvolysis of a mixture of 5-bromo-3-n-butyl-4-methyl-2-p-toluenesulfonylpyrrole (4b) and 5-bromo-4-n-butyl-3-methyl-2-p-toluenesulfonyl-pyrrole (4a) in trifluoroacetic acid and water, a reaction designed to produce 5-p-toluenesulfonyl-3-pyrrolin-2-ones, e.g., 5a and 5b.
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Reference:
Pyrroline – Wikipedia,
,1-Pyrroline | C4H7N – PubChem