Extended knowledge of 4-(2,5-Dioxo-2,5-dihydro-pyrrol-1-yl)-benzoicacid

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Reactions of N-arylmaleimides with 3-amino-1,2,4-triazole and 2-aminobenzimidazole

Figure represented. The reaction of 3-amino-1,2,4-triazole (1) with N-arylmaleimides leads to azolopyrimidines 4 and 5. The 2-aminobenzimidazole (2) in the reaction with 3 gives the pyrimidobenzimidazoles 6. In similar conditions, the reaction of amine 2 with maleic anhydride (7) leads to formation of 2-oxo-1,2,3,4-tetrahydropyrimido[1,2-a]benzimidazole-4-carboxylic acid (8). The structures of 4, 5, 6, and 8 were proved by X-Ray and NOE NMR measurements. J. Heterocyclic Chem., (2011)

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Pyrroline – Wikipedia,
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Preparation and characterization of new carrier drug polymers based maleimide and its drug release behaviour

In this work, two new drug substituted monomers and new homogenous and heterogeneous polymers were synthesized loaded with medicinal properties to extend the controlled drug. The first step includes preparation of compound (F1) via reaction of maleic anhydride with 4-aminobenzoic acid. Then compound (F1) was converted to its corresponding acyl chloride derivative which reacted with amino drugs (sulfadiazine, chlordiazepoxide) afforded (F2 and F3) monomers. Homogeneous polymers (F8 and F9) prepared through polymerization reaction of free radicals of the monomers (F2 and F3) under nitrogen using methyl ethyl ketone peroxide (MEKP) as initiator. Heterogeneous polymers (F14 and F15) prepared through polymerization reaction of free radicals of the monomers (F2 and F3) separately with acrylic acid under nitrogen using methyl ethyl ketone peroxide (MEKP) as initiator. All these prepared monomers and polymers were characterized by FT-IR and 1H NMR, 13C NMR spectroscopies. Controlled drug release and swelling % was studied in different pH values at 37 oC. Intrinsic viscosities were measured at 25 oC with Ostwald viscometer and applied the characteristic of solubility for these polymers.

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Sometimes chemists are able to propose two or more mechanisms that are consistent with the available data. COA of Formula: C11H7NO4, If a proposed mechanism predicts the wrong experimental rate law, however, the mechanism must be incorrect.Welcome to check out more blogs about 17057-04-4, in my other articles.

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P(N-Phenylmaleimide-Alt-Styrene) introduced with 4-carboxyl and its effect on the heat deflection temperature of nylon 6

P(N-phenylmaleimide-alt-styrene) (P(NPMI-alt-St)) and P(N-(4-carboxyphenyl)maleimidealt- styrene) (P(CPMI-alt-St)) were designed and synthesized via free radical copolymerization. Fourier transform infrared spectroscopy (FT-IR), nuclear magnetic resonance spectroscopy (1H NMR and 13C NMR), gel permeation chromatography (GPC), and differential scanning calorimetry (DSC) were used to confirm the structure of P(NPMI-alt-St) and P(CPMI-alt-St). Next, the effect of P(CPMI-alt-St) on the heat deflection temperature (HDT) of nylon 6 was studied. In comparison to the PA6/P(NPMI-alt-St) blend, with the addition of 10 wt %, the HDT value of the PA6/P(CPMI-alt-St) blend increased by 15.7 C, and the glass transition temperature (Tg) by Dynamic mechanical analysis (DMA) increased 2.3 C. According to the analysis of DMA, dynamic viscosity, and the SEM of PA6 and its blends, P(CPMI-alt-St) promoted its compatibility with PA6, and promoted the storage modulus and dynamic viscosity of the blends. Thus, the introduction of 4-carboxyl can significantly improve the effect of P(CPMI-alt-St) on the heat resistance modification of nylon 6.

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Pyrroline – Wikipedia,
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Simple exploration of 4-(2,5-Dioxo-2,5-dihydro-pyrrol-1-yl)-benzoicacid

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COPOLYMER AND PREPARATION METHOD THEREFOR

The present invention relates to a copolymer including 20 to 65 wt% of units derived from an alkyl styrene-based monomer; 10 to 40 wt% of units derived from a (meth)acrylate-based monomer; and 20 to 40 wt% of units derived from an aromatic vinyl-based monomer, based on the total weight of the copolymer, wherein the residual monomer content is 780 ppm or less, and a method for preparing the same.

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Pyrroline – Wikipedia,
1-Pyrroline | C4H7N – PubChem

Brief introduction of 4-(2,5-Dioxo-2,5-dihydro-pyrrol-1-yl)-benzoicacid

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Studying the sol-gel transition of styrene-divinyl benzene crosslinking co-polymerization via excimer forming dye molecules

A novel method based on the steady state fluorescence technique was used to study the sol-gel transition in the free radical crosslinking reaction between styrene (St) and divinyl benzene (DVB) with 2,2?-azobisisobutyronitrile (AIBN) as initiator. N-(4-(pyrenyl methylene)-oxycarbonyl phenyl)maleimide (Py-MI) was used as a fluorescence probe. The possible enchainment of Py-MI in alternating sequences occurred randomly in polymer clusters produced modifications in the fluorescence spectra, namely the shift at the higher wavelengths due to the excimer formation. The fluorescence spectra of Py-MI’s excimers allowed both to monitor the sol-gel transition and to test the critical exponents as function of co-monomer’s concentration. The gel fraction exponent beta and the weight average degree of polymerization exponent gamma agreed best with the static percolation values. Although this technique was applied for St-DVB co-polymerization, it may be generalized for the other monomers that are able to bind chemically to Py-MI monomer during the polymerization.

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Pyrroline – Wikipedia,
1-Pyrroline | C4H7N – PubChem

Simple exploration of 4-(2,5-Dioxo-2,5-dihydro-pyrrol-1-yl)-benzoicacid

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Synthesis and evaluation of novel 4-[(3H,3aH,6aH)-3-phenyl)-4,6-dioxo-2- phenyldihydro-2H-pyrrolo[3,4-d]isoxazol-5(3H,6H,6aH)-yl]benzoic acid derivatives as potent acetylcholinesterase inhibitors and anti-amnestic agents

The present study was designed to synthesize and evaluate pyrrolo-isoxazole benzoic acid derivatives as potential acetylcholinesterase (AChE) inhibitors for the management of Alzheimer’s disease. The synthesis of pyrrolo-isoxazole benzoic acid derivatives involved ring opening cyclization of p-aminobenzoic acid with maleic anhydride to yield maleanilic acid, which in turn afforded N-arylmaleimide via ring closed cyclization. Azomethine-N-oxides were obtained by condensation of N-arylhydroxylamine with differently substituted benzaldehydes followed by refluxing of N-arylmaleimide with differently substituted azomethine-N-oxides to pyrrolo-isoxazole benzoic acid derivatives as cis- and trans-stereoisomers. The synthesized compounds were evaluated in vitro for AChE inhibitory activity in rat brain homogenate with donepezil as standard AChE inhibitor. Thereafter, the most potent test compound was evaluated for in vitro butyrylcholinesterase inhibitory activity and in vivo memory evaluation in scopolamine (0.4 mg/kg)-induced amnesia in mice by employing Morris water maze test. All pyrrolo-isoxazole benzoic acid derivatives demonstrated potent AChE inhibitory activity. Most of compounds exhibited similar activity to donepezil and four of them (7h, 7i, 8i, and 8h, IC50 = 19.1 ¡À 1.9-17.5 ¡À 1.5 nM) displayed higher inhibitory activity as compared to donepezil (21.5 ¡À 3.2 nM) with compound 8ia (IC50 = 17.5 ¡À 1.5 nM) being the most active one. The test compound 8ia also ameliorated scopolamine-induced amnesia in mice in terms of restoration of time spent in target quadrant (TSTQ) and escape latency time (ELT). It may be concluded that pyrrolo-isoxazole benzoic acid derivatives may be employed as potential AChE inhibitors.

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Pyrroline – Wikipedia,
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New explortion of 4-(2,5-Dioxo-2,5-dihydro-pyrrol-1-yl)-benzoicacid

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Radical copolymerization of functional N-substituted maleimides with N-vinyl-2-pyrrolidone

Two functional N-substituted maleimide monomers, namely N-(4-carboxyphenyl)maleimide (CPMI) and N-(4-formylphenoxy-4?- carbonylphenyl) maleimide (FCPMI), were copolymerized with N Vinyl-2-pyrrolidone (NVP) at 90 C in the presence of 2,2?-azobisisobutyronitrile as initiator in dimethylformamide. The monomers reactivity ratios were calculated by extended Kelen-Tu?do?s and Mao-Huglin methods. The average reactivity ratios and Alfrey-Price Q and e Values were found to be r1 = 0.028, r2 = 0.347, Q1 = 0.035, e1 = 1.013 for CPMI/NVP system and r1 = 0.044, r2 = 0.060, Q1 = 0.145, e1 = 1.297 for the FCPMI/NVP system. The distribution of monomer sequences along the copolymer chain was calculated using a statistical method based on the obtained reactivity ratios. The thermal properties of the resulting copolymers were also investigated. These copolymers exhibit fairly high thermal stability with decomposition temperatures above 230 C. The effect of the N-substituents on the radical copolymerization of the above functional maleimides with NVP is discussed.

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Pyrroline – Wikipedia,
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Molecular modeling studies of N-substituted pyrrole derivatives-Potential HIV-1 gp41 inhibitors

2D-, 3D-QSAR and docking studies were carried out on 23 pyrrole derivatives, to model their HIV-1 gp41 inhibitory activities. The 2D, 3D-QSAR studies were performed using CODESSA software package and comparative molecular field analysis (CoMFA) technique, respectively. The CODESSA five-descriptor model has a correlation coefficient R2 = 0.825 and a standard deviation s2 = 0.132. The 3D-QSAR CoMFA study allowed to obtain a model showing a good correlative and predictive capability which statistical results, provided by a eight-component regression equation, are: R2 = 0.984, q2 = 0.463, s = 0.119. Docking studies were employed to determine probable binding conformation of these analogues into the gp41 active site using the AutoDock program whose results were found complementary with thus of 2D- and 3D-QSAR analysis. These findings provide guidance for the design and structural modifications of these derivatives for better anti-HIV-1 activity which is important for the development of a new class of entry inhibitors.

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Pyrroline – Wikipedia,
1-Pyrroline | C4H7N – PubChem

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Polyamide thermosets

The present invention provides (1) curable polyamide monomers represented by the formula: R1 -A1 -B1 -A2 -B2 -A3 -R2 where R1 and R2 are radicals selected from the group consisting of maleimide, substituted maleimide, nadimide, substituted nadimide, ethynyl, and (C(R3)2)2 where R3 is hydrogen with the proviso that the two carbon atoms of (C(R3)2)2 are bound on the aromatic ring of A1 or A3 to adjacent carbon atoms, A1 and A3 are 1,4-phenylene and the same where said group contains one or more substituents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro, lower alkyl, e.g., methyl, ethyl, and propyl, lower alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl or fluoroalkoxy, e.g., trifluoromethyl, pentafluoroethyl and the like, A2 is selected from the group consisting of 1,4-phenylene, 4,4′-biphenyl, 2,6-naphthylene and the same where said groups contain one or more substitutents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro, lower alkyl, e.g., methyl, ethyl, and propyl, lower alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl or fluoroalkoxy, e.g., trifluoromethyl, pentafluoroethyl and the like, and B1 and B2 are selected from the group consisting of –C(O)–N(H)– and –N(H)–C(O)–, (2) thermoset polyamide compositions comprised of cured segments derived from monomers represented by the formula: R1 -A1 -B1 -A2 -B2 -A3 -R2 as described above, and curable blends of at least two of the polyamide monomers and (4) processes of preparing the curable polyamide monomers.

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Pyrroline – Wikipedia,
1-Pyrroline | C4H7N – PubChem

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Sometimes chemists are able to propose two or more mechanisms that are consistent with the available data. Safety of 4-(2,5-Dioxo-2,5-dihydro-pyrrol-1-yl)-benzoicacid, If a proposed mechanism predicts the wrong experimental rate law, however, the mechanism must be incorrect.Welcome to check out more blogs about 17057-04-4, in my other articles.

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Synthesis and properties of phosphorus containing copoly(bismaleimide)

In this article, a phosphorus containing bismaleimide (V) based on 2- (6-oxido-6H-dibenz <1,2>6-yl)-1,4-dihydroxy phenylene (I) was synthesized and copolymerized with 4,4′-bismaleimidodiphenylmethane (BMDM) in various weight ratio (0-33 phr). DSC scans show that the introduction of V into BMDM has increased the processing window for the resulted copoly(bismaleimide). DMA scans show these cured BMIs exhibit good modulus (~ 2 GPa) up to 400C. There is no tangent peak for these cured BMIs implying that there is no relaxation below 400C. TMA scans show introduction of V into BMDM increase the coefficient of thermal expansion (CTE). However, CTE of these cured BMIs are less than 50 ppm, which is much less than common epoxy. There is no second transition during TMA heating scans up to 440C, so T(g)s of these cured BMIs are higher than 440C, which is consistent with the DMA measurement. TGA heating scans also indicate that they have high thermal stability and their char yields increase with the content of V. Char yields at 800C shift from 48 to 63 in nitrogen and from 0 to 18 in air when 25 phr of V was introduced into BMDM. TGA isothermal experiments show that these cured BMIs are thermally more stable in air than in nitrogen below 450C. Char yields also increase with the content of V. In this article, a phosphorus containing bismaleimide (V) based on 2-(6-oxido-6H-dibenz ?c,e? ?1,2?6-yl)-1,4-dihydroxy phenylene (I) was synthesized and copolymerized with 4,4?-bismaleimidodiphenylmethane (BMDM) in various weight ratio (0-33 phr). DSC scans show that the introduction of V into BMDM has increased the processing window for the resulted copoly(bismaleimide). DMA scans show these cured BMIs exhibit good modulus (approx. 2 GPa) up to 400C. There is no tangent peak for these cured BMIs implying that there is no relaxation below 400C. TMA scans show introduction of V into BMDM increase the coefficient of thermal expansion (CTE). However, CTE of these cured BMIs are less than 50 ppm, which is much less than common epoxy. There is no second transition during TMA heating scans up to 440C, so Tgs of these cured BMIs are higher than 440C, which is consistent with the DMA measurement. TGA heating scans also indicate that they have high thermal stability and their char yields increase with the content of V. Char yields at 800C shift from 48 to 63 in nitrogen and from 0 to 18 in air when 25 phr of V was introduced into BMDM. TGA isothermal experiments show that these cured BMIs are thermally more stable in air than in nitrogen below 450C. Char yields also increase with the content of V.

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Reference£º
Pyrroline – Wikipedia,
1-Pyrroline | C4H7N – PubChem